From:  Resmetirom and semaglutide in metabolic dysfunction-associated steatohepatitis (MASH): a comparative perspective

 Key physicochemical and pharmacological characteristics of resmetirom and semaglutide relevant to MASH therapy.

Parameter    Resmetirom (MGL-3196)    Semaglutide
Drug class/primary target    Selective THR-β agonist    Long-acting GLP-1 receptor agonist
CAS number    920509-32-6    910463-68-2
Molecular formula    C17H12Cl2N6O4    C187H291N45O59
Molecular weight    600.45 g·mol–1    4,113.58 g·mol–1
2-D structure    See Figure 1    See Figure 2
Physical appearance    White to off-white crystalline powder    White lyophilised powder (pen) or tablets (with SNAC)
Aqueous solubility (25°C)    < 0.1 mg·mL–1 (practically insoluble)    Highly soluble ≥ 1 mg·mL–1, pH ≈ 7.4
Solubility in DMSO/buffers    DMSO ≈ 45 mg·mL–1
    EtOH ≈ 2 mg·mL–1
    Fully soluble in isotonic aqueous buffers
LogP (cLogP)*    ≈ 4.8    n/a (large peptide)
pKa (dominant)    4.7 (carboxylic acid)    Multiple; isoelectric point ≈ 4.8
Formulation in trials    Immediate-release oral tablets 40/80/100 mg    Prefilled s.c. pens 0.25–2.4 mg; oral 3/7/14 mg (SNAC-enhanced)
Typical MASH study dose    80–100 mg orally once daily    0.4 mg s.c. daily (phase II); 2.4 mg s.c. weekly in obesity
Oral bioavailability    ≈ 30%    ≈ 1% (oral); s.c. ≈ 89%
Plasma protein binding    > 99%    > 99%
Elimination half-life    ≈ 35 h    ≈ 160 h (≈ 7 days)
Main metabolism/clearance    Hepatic oxidation & conjugation; biliary/fecal excretion    Proteolysis followed by β-oxidation; renal (54%) peptide fragments
Principal route(s) of administration    Oral    s.c.; oral (with SNAC)
Key therapeutic signals in MASH↓ MRI-PDFF, ↑ MASH resolution (≈ 30%), early fibrosis improvement    MASH resolution up to 59%, ≥ 13% weight loss, fibrosis signal weight-dependent
Most frequent adverse events    Mild pruritus, transient GI discomfort, reversible ↓ TSH    Nausea, vomiting, diarrhoea, gall-bladder events, and rare pancreatitis
Development status (mid-2024)    Licensed for use in non-cirrhotic MASH in March 2024 in the USA    Phase III ESSENCE-NASH ongoing; already marketed for T2DM & obesity
Representative trade names approved by the FDA    Rezdiffra (tablets)    Rybelsus (tablets), Ozempic (injection), Wegovy (injection)
Storage    2–8°C, protected from moisture/light    2–8°C (pens); room temperature ≤ 30°C for ≤ 56 days (in-use pens)
Mechanism of action    Hepatic    Systemic
Direct improvement of insulin resistance    No    Yes
Extra-hepatic benefits    Improves atherogenic dyslipidemia by strong LDL-C & ApoB lowering    Glycaemic & cardio-nephro-metabolic benefits

ApoB: apolipoprotein B; EtOH: ethanol; FDA: Food and Drug Administration; GI: gastrointestinal; GLP-1: glucagon-like peptide-1; LDL-C: low-density lipoprotein cholesterol; MASH: metabolic dysfunction-associated steatohepatitis; MRI-PDFF: magnetic resonance imaging-proton density fat fraction; NASH: nonalcoholic steatohepatitis; s.c.: subcutaneous; SNAC: sodium N-[8-(2-hydroxybenzoyl)amino] caprylate; T2DM: type 2 diabetes mellitus; THR-β: thyroid hormone receptor-β; TSH: thyroid-stimulating hormone. * LogP (cLogP) refers to the logarithm of the octanol-water partition coefficient, a measure of the fat-solubility of a drug.