Table Info

Table 3.

Compounds identified in fraction 2AFH50 via GC-MS

Components of 2AFH50	RT (min)	Qual %	Area %	MM (g/moL)
2,4-Di-tert-butylphenol	9.930	94	1.05	206.32
Tetradecanoic acid	12.808	97	1.59	228.37
2-Pentadecanone, 6,10,14-trimethyl-	13.585	80	1.29	268.50
n-Hexadecanoic acid	14.996	99	52.29	256.40
Heptadecanoic acid	15.763	91	1.42	270.45
13-Tetradece-11-yn-1-ol	16.107	59	1.37	208.34
1,6-Dimethyl-9-(1-methylethylidene)-5,12-dioxatricyclo[9.1.0.0(4,6)]dodecan-8-one	16.420	49^a	1.63	250.33
Octadecanoic acid	16.696	99	8.48	284.48
2,2,4a,6a,8a,9,12b,14a-Octamethyl-1,2,3,4,4a,5,6,6a,6b,7,8,8a,9,12,12a,12b,13,14,14a,14b-eicosahydropicene	17.218	46^a	1.58	410.70
Decanoic acid, 10-(2-hexylcyclopropyl)	17.429	99	10.78	296.49
1,4-Dioxaspiro[4.5]decane-6-carboxylic acid, dimethylamide	18.218	89	2.10	213.27
Cholesta-8,24-dien-3-ol, 4-methyl-, (3.beta.,4.alpha.)-	19.174	90	1.20	398.70
A-Norcholestan-3-one, 5-ethenyl-, (5.beta.)-	19.251	41^a	2.47	398.50
24S-Ethyl-5.alpha.-cholesta-2,22E-dien-6-one	20.784	64	5.26	410.70
Stigmasta-3,5-dien-7-one	21.273	70	5.41	410.68
2H-3,9a-methano-1-benzoxepin, octahydro-2,2,5a,9-tetramethyl-[3R-(3.alpha.,5a.alpha.,9.alpha.,9a.alpha.)]-	21.462	50	2.07	222.37

Area %: area percent, which corresponds to the proportion of each component in the fraction; Qual %: quality of fragment ion peak matching between the unknown component and suggested compounds from NIST14.L; RT: retention time in min; MM: molecular mass. The “a” in superscript represents suggested compounds from NIST14.L which have Qual % less than 50%

Declarations

Acknowledgments

The Centre for Natural Products Discovery (CNPD), School of Pharmacy and Biomolecular Sciences, Liverpool John Moores University, UK is gratefully acknowledged for the access to instruments, resources, and training provided BEA while he conducted the research at the centre as a visiting PhD student between June and October 2019, hosted by AAF and supervised by AAF, SDS and DWS.

Author contributions

BEA: Data curation, Formal analysis, Funding acquisition, Investigation, Methodology, Validation, Visualization, Writing—original draft, Writing—review & editing. BO: Conceptualization, Supervision, Writing—review & editing. JBM: Conceptualization, Supervision, Writing—review & editing. DWS: Formal analysis, Investigation, Methodology, Supervision, Validation, Writing—review & editing. SDS: Methodology, Resources, Supervision, Validation, Writing—review & editing. AAF: Conceptualization, Data curation, Formal analysis, Funding acquisition, Investigation, Methodology, Project administration, Resources, Supervision, Validation, Visualization, Writing—review & editing. All authors read and approved the manuscript.

Conflicts of interest

The authors declare that they have no conflicts of interest.

Ethical approval

Not applicable.

Consent to participate

Not applicable.

Consent to publication

Not applicable.

Availability of data and materials

Datasets are available from the authors upon reasonable request. Contact tobitune@yahoo.com or A.A.Fatokun@ljmu.ac.uk.

Funding

The work described in this manuscript was partly supported by a Seed Corn Grant (2017) awarded to AAF by Liverpool John Moores University (LJMU). This funder had no role in study design, data collection and analysis, decision to publish, or preparation of the manuscript.

Copyright

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